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How to make the gel

This version was saved 15 years, 1 month ago View current version     Page history
Saved by Nancie Ravenel
on February 26, 2009 at 8:59:20 am
 

To make the gel you measure out the appropriate amount of pemulen TR2 powder and mix with an appropriate amount of solvent.

 

The information page from Noveon includes information on relative base strength parts per 1 part Pemulen.


The master recipe Shelburne has used for the gel is

100 mL de-I water

10mL  base

1 g. Pemulen TR2


At Shelburne, we have used two alkaline compounds to make up the gel: triethanolamine (TEA) and a solution of 2% Tris(hydroxymethyl)aminomethane (TRIS) in deionized water.  Making the gel up with TEA using this recipe results in a gel with a pH of about 7.5-8.  When this gel proves to produce an emulsion that is too aggressive for cleaning, the gel recipe is modified replacing some of the TEA with the solution of 2% TRIS, a weaker base than TEA.  This often results in a less aggressive emulsion cleaner even though the pH remains at 7.5-8.

 

The first step in preparing the gel is to mix the water and the base together.  Then Pemulen powder is added slowly with constant stirring.  While we initially had used a magnetic stirrer to create the gel, Laura Brill found that stirring the Pemulen powder into the water by hand using a miniature balloon wisk created a smoother gel from the beginning. 

 

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